4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline synthesis

7synthesis methods

Product Name:4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline
CAS Number:2871-86-5
Molecular formula:C22H19N
Molecular Weight:297.39

1,1'-Biphenyl, 2-bromo-2'-(bromomethyl)-

13379-29-8
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Benzenesulfonicacid, 4-methyl-, 2-[[4-(dimethylamino)phenyl]methylene]hydrazide

18708-16-2
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4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline

2871-86-5
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Yield:2871-86-5 85%

Reaction Conditions:

with tris-(dibenzylideneacetone)dipalladium⁽⁰⁾;trifuran-2-yl-phosphane;caesium carbonate;lithium tert-butoxide in 1,4-dioxane at 120; for 12 h;Inert atmosphere;Sealed tube;

References:

Paraja, Miguel;Valdés, Carlos [Organic Letters,2017,vol. 19,# 8,p. 2034 - 2037] Location in patent:supporting information

86-73-7 Synthesis

86-73-7
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100-10-7 Synthesis

100-10-7
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$5.00/1g

2871-86-5
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References

251320-87-3
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2871-86-5
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References

1940-57-4
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$15.00/1g

2871-86-5
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References

Phosphonium, tributyl-9H-fluoren-9-yl-, bromide

7293-68-7
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2871-86-5
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References