ChemicalBook CAS DataBase List 4,4,5,5-TETRAMETHYL-2-(4-TERT-BUTYL-1-CYCLOHEXEN-1-YL)-1,3,2-DIOXABOROLANE

4,4,5,5-TETRAMETHYL-2-(4-TERT-BUTYL-1-CYCLOHEXEN-1-YL)-1,3,2-DIOXABOROLANE synthesis

4synthesis methods

Product Name:4,4,5,5-TETRAMETHYL-2-(4-TERT-BUTYL-1-CYCLOHEXEN-1-YL)-1,3,2-DIOXABOROLANE
CAS Number:287944-06-3
Molecular formula:C16H29BO2
Molecular Weight:264.21

4-tert-butyl-1-cyclohexen-1-yl trifluoromethanesulfonate

77412-96-5
4 suppliers
inquiry

73183-34-3
564 suppliers
$6.00/5g

4,4,5,5-TETRAMETHYL-2-(4-TERT-BUTYL-1-CYCLOHEXEN-1-YL)-1,3,2-DIOXABOROLANE

287944-06-3
59 suppliers
$119.00/1g

Yield:287944-06-3 94%

Reaction Conditions:

with triphenylphosphine;bis(triphenylphosphine)palladium(II) chloride in toluene;mixt. in toluene stirred at 50°C for 3 h; treated (H2O) at room temp.; extd. (benzene); washed with brine; dried (MgSO4); purified by chromy. on silica gel or by distn. (vac.);

References:

Takagi, Jun;Takahashi, Kou;Ishiyama, Tatsuo;Miyaura, Norio [Journal of the American Chemical Society,2002,vol. 124,# 27,p. 8001 - 8006]

61676-62-8 Synthesis

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

61676-62-8
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$11.19/5G

N'-(4-tert-butylcyclohexylidene)-4-Methylbenzenesulfonohydrazide

41780-53-4
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287944-06-3
59 suppliers
$119.00/1g

References

77412-96-5
4 suppliers
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25015-63-8
218 suppliers
$22.39/5G

287944-06-3
59 suppliers
$119.00/1g

References

98-53-3 Synthesis

98-53-3
275 suppliers
$5.00/1g

287944-06-3
59 suppliers
$119.00/1g

References