1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-hexadecachloro-29H,31H-phthalocyanine synthesis

2synthesis methods

Product Name:1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-hexadecachloro-29H,31H-phthalocyanine
CAS Number:28888-81-5
Molecular formula:C32H2Cl16N8
Molecular Weight:1065.66

117-08-8 Synthesis

Yield:28888-81-5 25%

Reaction Conditions:

with toluene-4-sulfonic acid;1,1,1,3,3,3-hexamethyl-disilazane in N,N-dimethyl-formamide at 150; for 10 h;

References:

Uchida, Hitoshi;Yoshiyama, Hideyuki;Reddy, Paidi Yella;Nakamura, Shuichi;Toru, Takeshi [Synlett,2003,# 13,p. 2083 - 2085]

1571-13-7 Synthesis