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1-(p-Chlorophenyl)-2,8,9-trioxa-5-aza-1-silabicyclo[3.3.3]undecane synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: LiAlH4 / diethyl ether / Heating
2: dicobalt octacarbonyl / CH2Cl2 / Ambient temperature

References:

Hosomi, Akira;Iijima, Susumu;Sakurai, Hideki [Chemistry Letters,1981,p. 243 - 246]