29276-11-7 synthesis
- Product Name:29276-11-7
- CAS Number:29276-11-7
- Molecular formula:C8H16ClOP
- Molecular Weight:194.64
107-40-4
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29276-11-7
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Yield:29276-11-7 92%
Reaction Conditions:
Stage #1: 2,4,4-trimethylpent-2-enewith Aluminum Chloride;phosphorus trichloride in dichloromethane at 0; for 2.16667 h;Inert atmosphere;Schlenk technique;
Stage #2: with lithium hydroxide monohydrate in dichloromethane; for 0.5 h;Inert atmosphere;Schlenk technique;
References:
Nykaza, Trevor V.;Harrison, Tyler S.;Ghosh, Avipsa;Putnik, Rachel A.;Radosevich, Alexander T. [Journal of the American Chemical Society,2017,vol. 139,# 20,p. 6839 - 6842] Location in patent:supporting information
7116-86-1
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29276-11-7
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