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ChemicalBook CAS DataBase List Carbamic acid, [(1R)-1,2-dimethylpropyl]-, 1,1-dimethylethyl ester (9CI)

Carbamic acid, [(1R)-1,2-dimethylpropyl]-, 1,1-dimethylethyl ester (9CI) synthesis

3synthesis methods
(S)-1-Iodo-2-(Boc-amino)-3-methylbutane

161529-21-1
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Carbamic acid, [(1R)-1,2-dimethylpropyl]-, 1,1-dimethylethyl ester (9CI)

293305-73-4
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Yield:293305-73-4 92%

Reaction Conditions:

with sodium tri-sec-butylborohydride in tetrahydrofuran at 5; for 1.5 h;Reduction;

References:

Quagliato, Dominick A.;Andrae, Patrick M.;Matelan, Edward M. [Journal of Organic Chemistry,2000,vol. 65,# 16,p. 5037 - 5042]