1(2H)-Naphthalenone, 2-fluoro-3,4-dihydro-7-methoxy- synthesis

1synthesis methods

Product Name:1(2H)-Naphthalenone, 2-fluoro-3,4-dihydro-7-methoxy-
CAS Number:295779-87-2
Molecular formula:C11H11FO2
Molecular Weight:194.2

6836-19-7
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1(2H)-Naphthalenone, 2-fluoro-3,4-dihydro-7-methoxy-

295779-87-2
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Yield:295779-87-2 85%

Reaction Conditions:

Stage #1: 7-Methoxy-1-tetralonewith methanol;1-fluoro-4-hydroxy-1,4-diazoniabicyclo[2.2.2]octane bis(tetrafluoroborate) in acetonitrile;Fluorination;Ketalization;
Stage #2: with hydrogenchloride in acetonitrile;Further stages.;Hydrolysis;

References:

Stavber, Stojan;Jereb, Marjan;Zupan, Marko [Chemical Communications,2000,# 14,p. 1323 - 1324]