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2H-[1,3]Thiazino[3,2-a]benzimidazole(8CI,9CI) synthesis

7synthesis methods
51389-04-9 Synthesis
1H-Benzimidazole,2-(2-propenylthio)-(9CI)

51389-04-9
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2H-[1,3]Thiazino[3,2-a]benzimidazole, 3-bromo-3,4-dihydro-

167708-19-2
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Yield:167708-19-2 76%

Reaction Conditions:

with bromine;sodium acetate in N,N-dimethyl-formamide at 80; for 5 h;

References:

Korotkikh, N. I.;Raenko, G. F.;Shvaika, O. P. [Chemistry of Heterocyclic Compounds,1995,vol. 31,# 3,p. 359 - 363][Khimiya Geterotsiklicheskikh Soedinenii,1995,# 3,p. 410 - 415]