(2S,3S)-3-AMINO-2-HYDROXY-4-PHENYL-BUTYRIC ACID synthesis

13synthesis methods

Product Name:(2S,3S)-3-AMINO-2-HYDROXY-4-PHENYL-BUTYRIC ACID
CAS Number:62023-59-0
Molecular formula:C18H19NO5
Molecular Weight:329.35

59830-60-3
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(2S,3S)-3-AMINO-2-HYDROXY-4-PHENYL-BUTYRIC ACID

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 95 percent / p-toluenesulphonic acid / CH₂Cl₂ / Heating
2: BF₃*Et₂O / CH₂Cl₂ / 2 h / Ambient temperature
3: 1.) pyridinium chlorochromate; 2.) HCl / 2.) Et₂O, 4 deg C, 24 h
4: NaOH / dioxane; H₂O

References:

Herranz, Rosario;Castro-Pichel, Julia;Vinuesa, Soledad;Garcia-Lopez, Ma. Teresa [Journal of the Chemical Society. Chemical communications,1989,# 14,p. 938 - 939]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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62023-59-0
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References

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62023-60-3 Synthesis

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62023-59-0
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References

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62023-59-0
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References

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62023-59-0
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References

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