3-([1,1-BIPHENYL]-4-YL)PROPIOLIC ACID synthesis
- Product Name:3-([1,1-BIPHENYL]-4-YL)PROPIOLIC ACID
- CAS Number:32340-38-8
- Molecular formula:C15H10O2
- Molecular Weight:222.24
124-38-9
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Yield:32340-38-8 96%
Reaction Conditions:
Stage #1: carbon dioxide;4-biphenylylacetylenewith Cs2CO3 in (methylsulfinyl)methane at 40; under 760.051 Torr; for 20 h;Inert atmosphere;Schlenk technique;
Stage #2: with hydrogenchloride in lithium hydroxide monohydrate;(methylsulfinyl)methane;
References:
Shi, Kai;Lu, Chengrong;Zhao, Bei [New Journal of Chemistry,2022,vol. 46,# 35,p. 16998 - 17003] Location in patent:supporting information
1030-07-5
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32340-38-8
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1591-31-7
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