3-(2,4-Dichlorophenyl)-2-propen-1-ol synthesis

3synthesis methods

Product Name:3-(2,4-Dichlorophenyl)-2-propen-1-ol
CAS Number:1504-59-2
Molecular formula:C9H8Cl2O
Molecular Weight:203.07

874-42-0
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1504-59-2
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) NaCH₂SOCH₃ / 1.) DMSO, RT, 30 min, 2.) DMSO, RT, 1 h
2: diethyl ether; methanol
3: DIBAL-H / CH₂Cl₂ / 0.5 h / 0 °C

References:

Gribble, Andrew D.;Dolle, Roland E.;Shaw, Antony;McNair, David;Novelli, Riccardo;Novelli, Christine E.;Slingsby, Brian P.;Shah, Virendra P.;Tew, David;Saxty, Barbara A.;Allen, Mark;Groot, Pieter H.;Pearce, Nigel;Yates, John [Journal of Medicinal Chemistry,1996,vol. 39,# 18,p. 3569 - 3584]

2-Propenoic acid, 3-(2,4-dichlorophenyl)-, ethyl ester

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References

3-(2,4-Dichloro-phenyl)-acrylic acid methyl ester

42174-01-6
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References