![](/CAS/GIF/4767-00-4.gif)
3-(2-BENZOTHIAZOLYLTHIO)PROPIONIC ACID synthesis
- Product Name:3-(2-BENZOTHIAZOLYLTHIO)PROPIONIC ACID
- CAS Number:4767-00-4
- Molecular formula:C10H9NO2S2
- Molecular Weight:239.31
Yield: 100%
Reaction Conditions:
Stage #1:2-Mercaptobenzothiazole with potassium carbonate in tetrahydrofuran for 0.166667 h;Inert atmosphere;
Stage #2:3-Bromopropionic acid in tetrahydrofuran at 20;Inert atmosphere;
Steps:
Compound 3 was obtained in quantitative yield as an off-whitesolid. 2-Marcaptobenzothiazol (670 mg) was dissolved in THF(10 mL), potassium carbonate (1.1 g) was added, and the reaction wasstirred for 10 min under argon. Then 3-bromoproponic acid (910 mg)was added. The reaction was allowed to stir overnight at room temperatureunder argon. The reaction was neutralized with 2 M HCl and theproduct was extracted with DCM.
References:
Berkman, Clifford E.;Chen, Wei;Knight, Jessica Renee;Wang, Yingying;Xian, Ming;Xu, Shi [Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy,2021,vol. 247,art. no. 119072]
![2-Oxetanone](/CAS/GIF/57-57-8.gif)
57-57-8
156 suppliers
$24.73/250mgs:
![Sodium mercaptobenzothiazole](/CAS/GIF/2492-26-4.gif)
2492-26-4
207 suppliers
$11.00/5g
![3-(2-BENZOTHIAZOLYLTHIO)PROPIONIC ACID](/CAS/GIF/4767-00-4.gif)
4767-00-4
63 suppliers
$7.00/5g
![Propanenitrile, 3-(2-benzothiazolylthio)- (9CI)](/CAS/GIF/25176-72-1.gif)
25176-72-1
4 suppliers
$144.00/1ea
![3-(2-BENZOTHIAZOLYLTHIO)PROPIONIC ACID](/CAS/GIF/4767-00-4.gif)
4767-00-4
63 suppliers
$7.00/5g
![2-Mercaptobenzothiazole](/CAS/GIF/149-30-4.gif)
149-30-4
627 suppliers
$5.00/25g
![Acrylic acid](/CAS/GIF/79-10-7.gif)
79-10-7
687 suppliers
$20.16/100 mL
![3-(2-BENZOTHIAZOLYLTHIO)PROPIONIC ACID](/CAS/GIF/4767-00-4.gif)
4767-00-4
63 suppliers
$7.00/5g
![2-Mercaptobenzothiazole](/CAS/GIF/149-30-4.gif)
149-30-4
627 suppliers
$5.00/25g
![3-(2-BENZOTHIAZOLYLTHIO)PROPIONIC ACID](/CAS/GIF/4767-00-4.gif)
4767-00-4
63 suppliers
$7.00/5g