ChemicalBook CAS DataBase List [3-(2-Ethylhexyl)-2-thienyl]tributylstannane

[3-(2-Ethylhexyl)-2-thienyl]tributylstannane synthesis

4synthesis methods

Product Name:[3-(2-Ethylhexyl)-2-thienyl]tributylstannane
CAS Number:1235512-21-6
Molecular formula:C24H46SSn
Molecular Weight:485.4

[3-(2-Ethylhexyl)-2-thienyl]tributylstannane

1235512-21-6
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4,6-bis(3'-(2-ethylhexyl)thien-2'-yl)thieno[3,4-c][1,2,5]thiadiazole

1314359-43-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 3 h / Inert atmosphere; Reflux
2.1: formic acid; zinc / dichloromethane / 0.58 h / Reflux
3.1: pyridine; N-phenylsulfinylamine / 0.08 h / 80 °C / Inert atmosphere
3.2: 1 h

References:

Cimrova, Vera;Kminek, Ivan;Pavlackova, Petra;Vyprachticky, Drahomir [Journal of Polymer Science, Part A: Polymer Chemistry,2011,vol. 49,# 15,p. 3426 - 3436]

1235512-21-6
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1314359-44-8 Synthesis

4,6-bis(5'-bromo-3'-(2-ethylhexyl)thien-2'-yl)thieno[3,4-c][1,2,5]thiadiazole

1314359-44-8
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References

1235512-21-6
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8,10-bis(3-(2-ethylhexyl)thiophen-2-yl)trithieno[3,4-b:3',2'-f:2'',3''-h]quinoxaline

1235512-25-0
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References

1235512-21-6
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8,10-bis(5-bromo-3-(2-ethylhexyl)thiophen-2-yl)trithieno[3,4-b:3',2'-f:2'',3''-h]quinoxaline

1235512-28-3
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References