3-(2-hydroxyethyl)benzene-1,2-diol synthesis

Yield:62978-84-1 68%

Reaction Conditions:

Stage #1: 2-(2-hydroxyphenyl)ethanolwith carbonic acid dimethyl ester at 20; for 1 h;
Stage #2: with sodium dithionite in water at 20; for 0.0833333 h;chemoselective reaction;

References:

Bernini, Roberta;Crisante, Fernanda;Barontini, Maurizio;Tofani, Daniela;Balducci, Valentina;Gambacorta, Augusto [Journal of Agricultural and Food Chemistry,2012,vol. 60,# 30,p. 7408 - 7416] Location in patent:experimental part