ChemicalBook CAS DataBase List 3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE

3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE synthesis

5synthesis methods

Product Name:3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE
CAS Number:91969-32-3
Molecular formula:C11H14O
Molecular Weight:162.23

820-71-3 Synthesis

820-71-3
99 suppliers
$13.00/1g

578-57-4
300 suppliers
$6.00/10g

91969-32-3
9 suppliers
$252.00/1g

Yield:91969-32-3 79%

Reaction Conditions:

with pyridine;nickel(II) iodide;4-chloro-2-(4,5-dihydro-1H-imidazol-2-yl)pyridine;tetrabutylammomium bromide;magnesium chloride;zinc in N,N-dimethyl acetamide at 60; for 12 h;Schlenk technique;Inert atmosphere;regioselective reaction;

References:

Cui, Xiaozhan;Wang, Shulin;Zhang, Yuwei;Deng, Wei;Qian, Qun;Gong, Hegui [Organic and Biomolecular Chemistry,2013,vol. 11,# 19,p. 3094 - 3097] Location in patent:supporting information