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3-(2-NAPHTHYL)-1-PHENYL-1H-PYRAZOLE-4-CARBALDEHYDE synthesis

9synthesis methods
Methanesulfonic acid, 1,1,1-trifluoro-, 4-formyl-1-phenyl-1H-pyrazol-3-yl ester

1354413-51-6
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32316-92-0 Synthesis
2-Naphthaleneboronic acid

32316-92-0
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$6.00/1g

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Yield:36640-53-6 79%

Reaction Conditions:

with potassium phosphate;tetrakis(triphenylphosphine) palladium(0);potassium bromide in 1,4-dioxane; for 3 h;Inert atmosphere;Reflux;Suzuki-Miyaura cross-coupling reaction;

References:

Arbaciauskiene, Egle;Martynaitis, Vytas;Krikstolaityte, Sonata;Holzer, Wolfgang;Sackus, Algirdas [ARKIVOC,2011,vol. 2011,# 11,p. 1 - 21] Location in patent:experimental part