3-(2H-1,2,3-triazol-4-yl)aniline synthesis
- Product Name:3-(2H-1,2,3-triazol-4-yl)aniline
- CAS Number:876343-39-4
- Molecular formula:C8H8N4
- Molecular Weight:160.18
54060-30-9
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Yield:876343-39-4 19%
Steps:
7 Preparation of 3-(1H-1,2,3-triazol-4-yl)-phenylamine
Example 7 Preparation of 3-(1H-1,2,3-triazol-4-yl)-phenylamine Following the procedure of Example 1, except substituting 3-ethynyl-phenylamine for 3-ethynylphenol, the title compound was prepared as a tan solid (19%). 1H-NMR (400 MHz, CD3OD): δ 8.05 (s, 1H), 7.12-7.20 (m, 3H), 6.73-6.75 (m, 1H). MS (ESI) 161.2 (M+H)+.
References:
US2003/220371,2003,A1