3,3,3-TRIFLUOROPROPYLAMINE HYDROCHLORIDE synthesis
- Product Name:3,3,3-TRIFLUOROPROPYLAMINE HYDROCHLORIDE
- CAS Number:2968-33-4
- Molecular formula:C3H7ClF3N
- Molecular Weight:149.54
347190-33-4
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2968-33-4
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Yield:2968-33-4 80%
Reaction Conditions:
Stage #1:2-(3,3,3-trifluoropropyl)isoindoline-1,3-dione with sodium tetrahydroborate in water;isopropyl alcohol at 20; for 24 h;
Stage #2: with acetic acid at 0 - 80; for 2 h;
References:
Josse, Olivier;Labar, Daniel;Georges, Benoit;Grégoire, Vincent;Marchand-Brynaert, Jacqueline [Bioorganic and Medicinal Chemistry,2001,vol. 9,# 3,p. 665 - 675]