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ChemicalBook CAS DataBase List 3-(3,4,5-TRIFLUOROPHENYL)PROPIOPHENONE

3-(3,4,5-TRIFLUOROPHENYL)PROPIOPHENONE synthesis

3synthesis methods
936-59-4 Synthesis
3-Chloropropiophenone

936-59-4
431 suppliers
$8.00/5g

143418-49-9 Synthesis
3,4,5-Trifluorophenylboronic acid

143418-49-9
386 suppliers
$5.00/1g

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Yield:898777-56-5 87%

Reaction Conditions:

with potassium phosphate;Wilkinson's catalyst;2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl in 1,4-dioxane at 60; under 750.075 Torr; for 20 h;Inert atmosphere;

References:

Jiang, Quanbin;Guo, Tenglong;Wang, Qingfu;Wu, Ping;Yu, Zhengkun [Advanced Synthesis and Catalysis,2013,vol. 355,# 9,p. 1874 - 1880] Location in patent:supporting information