3,3''-dihexyl-2,2':5',2''-terthiophene synthesis

5synthesis methods

Product Name:3,3''-dihexyl-2,2':5',2''-terthiophene
CAS Number:135831-08-2
Molecular formula:C24H32S3
Molecular Weight:416.71

1693-86-3 Synthesis

1693-86-3
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135831-08-2
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: acetic acid; N-Bromosuccinimide / 24 h / 20 °C / Inert atmosphere
2.1: magnesium / diethyl ether; tetrahydrofuran / 1 h / Reflux; Inert atmosphere
2.2: 1.5 h / Reflux; Inert atmosphere

References:

Rakstys, Kasparas;Paek, Sanghyun;Gao, Peng;Gratia, Paul;Marszalek, Tomasz;Grancini, Giulia;Cho, Kyung Taek;Genevicius, Kristijonas;Jankauskas, Vygintas;Pisula, Wojciech;Nazeeruddin, Mohammad Khaja [Journal of Materials Chemistry A,2017,vol. 5,# 17,p. 7811 - 7815]

3141-27-3 Synthesis