3,3'-DIMETHYL-3''-METHYLTRITYL ALCOHOL synthesis
3synthesis methods
- Product Name:3,3'-DIMETHYL-3''-METHYLTRITYL ALCOHOL
- CAS Number:51226-48-3
- Molecular formula:C22H22O
- Molecular Weight:302.41
Yield:51226-48-3 93%
Reaction Conditions:
Stage #1: meta-bromotoluenewith n-butyllithium in tetrahydrofuran at -78; for 0.5 h;
Stage #2: Diethyl carbonate in tetrahydrofuran at -78 - 20;
References:
Thibeault, Dominic;Auger, Michele;Morin, Jean-Francois [European Journal of Organic Chemistry,2010,# 16,p. 3049 - 3067] Location in patent:experimental part
