3,3-Dimethyltricyclo[2.2.1.02,6]heptane synthesis

8synthesis methods

Product Name:3,3-Dimethyltricyclo[2.2.1.02,6]heptane
CAS Number:473-02-9
Molecular formula:
Molecular Weight:0

1-bromo-7,7-dimethylbicyclo[2.2.1]heptan-2-one

34252-16-9
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473-02-9
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 90 percent / LiAlH₄ / diethyl ether / 0 °C
2: 85 percent / pyridine
3: 1.) Mg^* / 1.) THF reflux ; 2.)MeOH
4: 17 percent / 760 °C / FVP (flash vacuum pyrolysis)

References:

Barton, Thomas J.;Yeh Ming-Hsiung [Tetrahedron Letters,1987,vol. 28,# 51,p. 6421 - 6424]

Bicyclo[2.2.1]heptan-2-ol, 1-bromo-7,7-dimethyl-, exo- (9CI)

54285-95-9
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473-02-9
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References

Silane, [(1-bromo-7,7-dimethylbicyclo[2.2.1]hept-2-yl)oxy]dimethyl-, exo- (9CI)

116417-14-2
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473-02-9
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References

Bicyclo[2.2.1]heptan-2-ol, 1-(dimethylsilyl)-7,7-dimethyl-, exo- (9CI)

116417-16-4
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473-02-9
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References

5957-68-6 Synthesis

5957-68-6
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529-16-8 Synthesis

529-16-8
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473-02-9
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References