3,3'-Dithiobis(N-octylpropionamide) synthesis
- Product Name:3,3'-Dithiobis(N-octylpropionamide)
- CAS Number:33312-01-5
- Molecular formula:C22H44N2O2S2
- Molecular Weight:432.73
Yield:33312-01-5 92%
Reaction Conditions:
with hydrogenchloride in water at 10; for 15 h;Temperature;
Steps:
1-4 Example 3
Add 200mL water and 1mL hydrochloric acid to a 500mL round bottom flask,At 10°C, 47.66g of dimethyl dithiodipropionate and 72.37g of n-octylamine were slowly added, and the reaction was stirred at this temperature for 15h. The solid was separated by centrifugation and washed with 50 mL water and 20 mL methanol,After drying for 12 hours, 79.62 g of white powder 3,3'-dithiodioctylpropionamide was obtained with a yield of 92%.
References:
CN113582941,2021,A Location in patent:Paragraph 0032-0034; 0036-0037; 0039-0040; 0042-0043
1119-62-6
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