3-(3-METHOXYPHENYL)-1-METHYLPIPERIDIN-3-AMINE synthesis

2synthesis methods

Product Name:3-(3-METHOXYPHENYL)-1-METHYLPIPERIDIN-3-AMINE
CAS Number:1236302-87-6
Molecular formula:C13H20N2O
Molecular Weight:220.31

53016-47-0
1 suppliers
inquiry

3-(3-METHOXYPHENYL)-1-METHYLPIPERIDIN-3-AMINE

1236302-87-6
4 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: Amberlyst A-21 / 1,4-dioxane / 20 °C
2.1: water; 1,4-dioxane / 0.08 h / 20 °C
2.2: 6 h / 65 °C
3.1: hydrogenchloride; zinc / water; 1,4-dioxane / 0.5 h / 20 °C
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / Reflux

References:

Pinard, Emmanuel;Alberati, Daniela;Alvarez-Sanchez, Ruben;Brom, Virginie;Burner, Serge;Fischer, Holger;Hauser, Nicole;Kolczewski, Sabine;Lengyel, Judith;Mory, Roland;Saladin, Christian;Schulz-Gasch, Tanja;Stalder, Henri [ACS Medicinal Chemistry Letters,2014,vol. 5,# 4,p. 428 - 433]

Benzenebutanoic acid, 3-methoxy-γ-nitro-, methyl ester

1558681-53-0
0 suppliers
inquiry

1236302-87-6
4 suppliers
inquiry

References