3-(3-METHOXYPHENYL)-2-METHYL-1-PROPENE synthesis
- Product Name:3-(3-METHOXYPHENYL)-2-METHYL-1-PROPENE
- CAS Number:68383-29-9
- Molecular formula:C11H14O
- Molecular Weight:162.23
820-71-3
95 suppliers
$13.00/1g
766-85-8
188 suppliers
$22.00/5g
6161-50-8
34 suppliers
$45.00/100mg
68383-29-9
10 suppliers
$252.00/1g
Yield:68383-29-9 61% ，6161-50-8 21 % Chromat.
Reaction Conditions:
Stage #1: methallyl acetatewith indium(III) chloride;N,N-dimethylbutylamine;lithium chloride;indium;tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide at 35;
Stage #2: 3-methoxy-1-iodobenzene in N,N-dimethyl-formamide at 100;
References:
Lee, Phil Ho;Seomoon, Dong;Lee, Kooyeon;Kim, Sundae;Kim, Hyunseok;Kim, Hyun;Shim, Eunkyong;Lee, Miae;Lee, Seokju;Kim, Misook;Sridhar, Madabhushi [Advanced Synthesis and Catalysis,2004,vol. 346,# 13-15,p. 1641 - 1645]