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898774-37-3

3-(3-METHOXYPHENYL)-2'-METHYLPROPIOPHENONE synthesis

1synthesis methods
39627-62-8 Synthesis
1-o-tolylprop-2-en-1-ol

39627-62-8
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α-[(1E)-2-(3-Methoxyphenyl)ethenyl]-2-methylbenzenemethanol

1370701-25-9
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Yield:1370701-25-9 58% ,898774-37-3 29%

Reaction Conditions:

with N-benzyl-N,N,N-triethylammonium chloride;palladium diacetate;sodium hydrogencarbonate in acetonitrile at 50; for 24 h;Inert atmosphere;regioselective reaction;Mizoroki-Heck reaction;

References:

Krishna;Reddy, A. Gopi Krishna;Ramulu, B. Venkat;Mahendar;Satyanarayana [Synlett,2012,# 3,p. 375 - 380] Location in patent:supporting information; experimental part