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ChemicalBook CAS DataBase List 3,4,6-Tri-O-benzoyl-D-glucal, 97%

3,4,6-Tri-O-benzoyl-D-glucal, 97% synthesis

8synthesis methods
-

Yield:13322-90-2 90%

Reaction Conditions:

Stage #1: D-glucal triacetatewith sodium methylate in methanol at 0; for 4 h;
Stage #2: benzoyl chloridewith pyridine at 0 - 20; for 5 h;

References:

Bi, Jingjing;Tan, Qiang;Wu, Hao;Liu, Qingfeng;Zhang, Guisheng [Organic Letters,2021,vol. 23,# 16,p. 6357 - 6361] Location in patent:supporting information