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ChemicalBook CAS DataBase List 3,4-Bis(octyloxy)benzoic acid

3,4-Bis(octyloxy)benzoic acid synthesis

11synthesis methods
Benzoic acid, 3,4-bis(octyloxy)-, methyl ester

367514-65-6
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3,4-Bis(octyloxy)benzoic acid

131525-56-9
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Yield:131525-56-9 99%

Reaction Conditions:

Stage #1: methyl 3,4-bis(octan-1-yloxy)benzoatewith potassium hydroxide in methanol;water; for 24 h;Reflux;
Stage #2: with hydrogenchloride in methanol;water;

References:

Hope-Ross, Kyle A.;Heiney, Paul A.;Kadla, John F. [Canadian Journal of Chemistry,2010,vol. 88,# 7,p. 639 - 645] Location in patent:supporting information; experimental part

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