3-(4-Bromo-phenoxy)-azetidine synthesis
- Product Name:3-(4-Bromo-phenoxy)-azetidine
- CAS Number:954224-25-0
- Molecular formula:C9H10BrNO
- Molecular Weight:228.09
960402-39-5
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954224-25-0
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Yield:954224-25-0 100%
Reaction Conditions:
with trifluoroacetic acid in dichloromethane at 20;
Steps:
8.2 3-(4-bromophenoxy)azetidine
To a solution of tert-butyl 3-(4-bromophenoxy)azetidine-1-carboxylate (300 mg, 0.90 mmol) in CH2Cl2 (5 mL) was added TFA (5 mL).
The mixture was stirred at room temperature overnight.
The reaction mixture was concentrated in vacuo to give 3-(4-bromophenoxy)azetidine (207 mg, 100%) as a yellow oil.
References:
US2013/267493,2013,A1 Location in patent:Paragraph 0732
106-41-2
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954224-25-0
16 suppliers
$594.00/1g