3-(4-CHLOROBENZOYL)THIOPHENE synthesis
- Product Name:3-(4-CHLOROBENZOYL)THIOPHENE
- CAS Number:896618-56-7
- Molecular formula:C11H7ClOS
- Molecular Weight:222.69
1446424-90-3
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Yield:896618-56-7 76%
Reaction Conditions:
Stage #1: tri(3-thienyl)aluminium;4-chlorobenzaldehydewith 3,3-dimethyl-butan-2-one at 20; for 3 h;Cooling with ice;Oppenauer Oxidation;
Stage #2: with trifluoroacetic acid at 20; for 48 h;
References:
Fu, Ying;Yang, Yanshou;Hügel, Helmut M.;Du, Zhengyin;Wang, Kehu;Huang, Danfeng;Hu, Yulai [Organic and Biomolecular Chemistry,2013,vol. 11,# 27,p. 4429 - 4432] Location in patent:supporting information