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(3,4-DIHYDRO-2H-BENZO[1,4]OXAZIN-3-YL)-METHANOL synthesis

4synthesis methods
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Yield:36884-17-0 84%

Reaction Conditions:

with palladium 10% on activated carbon;diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate in ethanol; for 12 h;Inert atmosphere;Reflux;

References:

Meng, Qing-Yuan;Liu, Qiang;Li, Jing;Xing, Rui-Guang;Shen, Xiao-Xia;Zhou, Bo [Synlett,2009,# 20,p. 3283 - 3286] Location in patent:experimental part