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ChemicalBook CAS DataBase List 3,4-Dihydro-9-phenyl-1(2H)-acridinone

3,4-Dihydro-9-phenyl-1(2H)-acridinone synthesis

4synthesis methods
-

Yield:17401-27-3 68%

Reaction Conditions:

with Cu(II) decorated on isoniazid functionalized silica coated Fe3O4 magnetic nanoparticles in ethanol at 60; for 2 h;Friedlaender Quinoline Synthesis;

Steps:

2.4. Preparation of quinolines

General procedure: 1.2 mmol a-CH-acid, 1.0 mmol 2-aminoaryl ketone, and 0.07 gnanocatalyst were poured in a bottom round flask containingethanol solvent, and were heated and vigorously stirred untilthe end of the reaction. Once the reaction was completed, understoodvia TLC technique, the nanocatalyst was decanted from thereaction mixture by a magnet, which was then washed withEtOH (about 5 mL). The final product was recrystallized by ethanoland stored for characterization. All products were knowncompounds characterized by their M.p. which was comparedwith literature reports.

References:

Lotfi, Shahram;Nikseresht, Ahmad;Rahimi, Nasrin [Polyhedron,2019,vol. 173,art. no. 114148]