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ChemicalBook CAS DataBase List 3-[(4-METHOXYPHENYL)METHYL]CYCLOHEXANONE
898785-44-9

3-[(4-METHOXYPHENYL)METHYL]CYCLOHEXANONE synthesis

1synthesis methods
-

Yield:898785-44-9 58%

Reaction Conditions:

with [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate;3-quinuclidinol in methanol;acetone at 30; for 24 h;Sealed tube;Irradiation;Inert atmosphere;Schlenk technique;

References:

Lima, Fabio;Sharma, Upendra K.;Grunenberg, Lars;Saha, Debasmita;Johannsen, Sandra;Sedelmeier, Joerg;Van der Eycken, Erik V.;Ley, Steven V. [Angewandte Chemie - International Edition,2017,vol. 56,# 47,p. 15136 - 15140][Angew. Chem.,2017,vol. 129,# 47,p. 15332 - 15336,5] Location in patent:supporting information