3-[(4-methoxyphenyl)methylene]phthalide synthesis
- Product Name:3-[(4-methoxyphenyl)methylene]phthalide
- CAS Number:4767-61-7
- Molecular formula:C16H12O3
- Molecular Weight:252.26
176910-67-1
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4767-61-7
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29910-92-7
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Yield:4767-61-7 84% ,29910-92-7 14%
Reaction Conditions:
with sodium chlorite;sodium dihydrogenphosphate;2-methyl-but-2-ene in tetrahydrofuran;water;tert-butyl alcohol at 0 - 90; for 16 h;regioselective reaction;
References:
Li, Jim;Chin, Elbert;Lui, Alfred S.;Chen, Lijing [Tetrahedron Letters,2010,vol. 51,# 45,p. 5937 - 5939] Location in patent:scheme or table