3-(4-METHYLPHENYL)-4'-TRIFLUOROMETHYLPROPIOPHENONE synthesis

1synthesis methods

Product Name:3-(4-METHYLPHENYL)-4'-TRIFLUOROMETHYLPROPIOPHENONE
CAS Number:898769-04-5
Molecular formula:C17H15F3O
Molecular Weight:292.3

1576-35-8 Synthesis

1576-35-8
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$10.00/1g

1-(4-(trifluoromethyl)phenyl)prop-2-en-1-ol

149946-79-2
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3-(4-METHYLPHENYL)-4'-TRIFLUOROMETHYLPROPIOPHENONE

898769-04-5
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$433.00/1g

Yield:898769-04-5 80%

Reaction Conditions:

with tetrabutylammomium bromide;oxygen;palladium diacetate in water;dimethyl sulfoxide;N,N-dimethyl-formamide at 120; under 760.051 Torr;Schlenk technique;Heck Reaction;

References:

Huang, Liangbin;Qi, Ji;Wu, Xia;Wu, Wanqing;Jiang, Huanfeng [Chemistry - A European Journal,2013,vol. 19,# 46,p. 15462 - 15466] Location in patent:supporting information