3,5-Dibromo-4-iodo-tert-butylbenzene synthesis
- Product Name:3,5-Dibromo-4-iodo-tert-butylbenzene
- CAS Number:172368-00-2
- Molecular formula:C10H11Br2I
- Molecular Weight:417.91
10546-67-5
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$30.00/5g
172368-00-2
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$420.00/5g
Yield:172368-00-2 95%
Reaction Conditions:
Stage #1: 2,6-dibromo-4-(tert-butyl)anilinewith sulfuric acid;sodium nitrite in acetic acid at 5 - 20; for 7 h;Inert atmosphere;Schlenk technique;
Stage #2: with iodine;potassium iodide in water;acetic acid at 20;Inert atmosphere;Schlenk technique;
References:
Zaffaroni, Riccardo;Bobylev, Eduard O.;Plessius, Raoul;Van Der Vlugt, Jarl Ivar;Reek, Joost N. H. [Journal of the American Chemical Society,2020,vol. 142,# 19,p. 8837 - 8847] Location in patent:supporting information
769-92-6
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$6.00/10g
172368-00-2
28 suppliers
$420.00/5g