3,5-DIBROMO-4-METHYLBENZONITRILE synthesis
- Product Name:3,5-DIBROMO-4-METHYLBENZONITRILE
- CAS Number:116596-20-4
- Molecular formula:C8H5Br2N
- Molecular Weight:274.94
67973-32-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C / Cooling with ice
2: ammonium hydroxide / tetrahydrofuran / 0.5 h / 20 °C
3: oxalyl dichloride; triethylamine; Triphenylphosphine oxide / dichloromethane / 0.5 h / 20 °C / Cooling with ice
References:
WO2021/254483,2021,A1
13194-73-5
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116596-20-4
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