3,5-Difluoro-benzenepropanaMine synthesis
- Product Name:3,5-Difluoro-benzenepropanaMine
- CAS Number:105219-40-7
- Molecular formula:C9H11F2N
- Molecular Weight:171.19
105219-39-4
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105219-40-7
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Yield:105219-40-7 98%
Reaction Conditions:
in methanol;
Steps:
F 3-(3,5-Difluorophenyl)propylamine
Example F 3-(3,5-Difluorophenyl)propylamine A solution of 3-(3,5-difluorophenyl)propyl azide in methanol (75 ml) and Raney nickel was shaken in a hydrogen atmosphere (50 pounds) for 5.5 hours. The catalyst was filtered and the solvent was removed under vacuum to give the product as an oil (4.94 g, 98%).
References:
EP323737,1989,A1
32085-88-4
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105219-40-7
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461-96-1
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$6.00/10g
105219-40-7
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