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ChemicalBook CAS DataBase List 3,5-Difluorobenzene-1-sulfonyl Fluoride

3,5-Difluorobenzene-1-sulfonyl Fluoride synthesis

2synthesis methods
21538-06-7 Synthesis
1,3,5-BENZENETRISULFONYL CHLORIDE

21538-06-7
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3,5-Difluorobenzene-1-sulfonyl Fluoride

115650-77-6
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 55 percent / ZnF2 / pyridine / 2 h
2: 49 percent / KF / tetrahydrothiophene 1,1-dioxide / 1.25 h / 190 - 210 °C

References:

Puy, Michael Van Der [Journal of Organic Chemistry,1988,vol. 53,# 18,p. 4398 - 4401]