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ChemicalBook CAS DataBase List 3,5-dihydroxy-4-ethylstilbene
79338-80-0

3,5-dihydroxy-4-ethylstilbene synthesis

4synthesis methods
-

Yield:79338-80-0 91%

Reaction Conditions:

with boron tribromide

Steps:

2 Experiment 18. 2-Ethyl-5-(2-phenylethenyl)-1,3-benzenediol (24B).

Experiment 18. 2-Ethyl-5-(2-phenylethenyl)-1,3-benzenediol (24B). This material was synthesised from 1-(3,5-dimethoxy-4-ethylphenyl)-2-phenylethene and BBr3 in 91% yield by the same method as described in example 6. 1H-NMR (CDCl3, ppm): δ 1.22 (t, J=7.5 Hz, 6H), 2.70 (q, J=7.5 Hz, 2H), 4.81 (s, 2H), 6.60 (s, 2H), 7.00 (s, 2H), 7.26 (m, 1H), 7.36 (m, 2H), 7.52 (m, 2H).

References:

US2005/59733,2005,A1