![](/CAS/20180703/GIF/5345-09-5.gif)
3,5-DIMETHYL-2-NITROPHENOL synthesis
- Product Name:3,5-DIMETHYL-2-NITROPHENOL
- CAS Number:5345-09-5
- Molecular formula:C8H9NO3
- Molecular Weight:167.16
![Pyridine, 2-(3,5-dimethylphenoxy)-](/CAS/20210305/GIF/28355-47-7.gif)
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5345-09-5
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: palladium diacetate; silver(I) nitrite; dipotassium peroxodisulfate / 1,2-dichloro-ethane / 48 h / 110 °C / Schlenk technique
2.1: methyl trifluoromethanesulfonate / toluene / 2 h / 100 °C / Inert atmosphere
2.2: 0.25 h / Reflux; Inert atmosphere
References:
Zhang, Wei;Zhang, Jian;Ren, Shaobo;Liu, Yunkui [Journal of Organic Chemistry,2014,vol. 79,# 23,p. 11508 - 11516]
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5345-09-5
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![3,5-Dimethylphenol](/CAS/GIF/108-68-9.gif)
108-68-9
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![3,5-DIMETHYL-2-NITROPHENOL](/CAS/20180703/GIF/5345-09-5.gif)
5345-09-5
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$45.00/1mg
![3,5-Dimethyl-4-nitrophenol](/CAS/GIF/5344-97-8.gif)
5344-97-8
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$10.00/250mg
![3,5-Dimethylphenol](/CAS/GIF/108-68-9.gif)
108-68-9
332 suppliers
$9.00/5g
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5345-09-5
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$45.00/1mg
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![3,5-DIMETHYL-2-NITROPHENOL](/CAS/20180703/GIF/5345-09-5.gif)
5345-09-5
8 suppliers
$45.00/1mg