![](/CAS/GIF/4110-35-4.gif)
3,5-Dinitrobenzonitrile synthesis
- Product Name:3,5-Dinitrobenzonitrile
- CAS Number:4110-35-4
- Molecular formula:C7H3N3O4
- Molecular Weight:193.12
The same authors also reported that alkyl, benzylic, aryl, and heteroaryl aldoximes bearing various functionalities could be readily converted to the corresponding nitriles using diphosgene in good yields of 82–96%.
![Benzenecarboximidic acid, 3,5-dinitro-, methyl ester](/CAS/20210305/GIF/86475-51-6.gif)
86475-51-6
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![3,5-Dinitrobenzonitrile](/CAS/GIF/4110-35-4.gif)
4110-35-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 83 percent / NH4Cl / methanol / 12 h / 55 - 60 °C
2: 7 percent / NaCl, NaOCl / dimethylsulfoxide; hexane; diethyl ether / 1.) 0 deg C, 1.5 h, 2.) room temp, 20 min.
3: NaN3, 2-nitropropane sodium salt / dimethylsulfoxide / 0.01 h / 17 °C
References:
Creary, Xavier [Journal of Organic Chemistry,1993,vol. 58,# 27,p. 7700 - 7708]
![3,5-Dinitrobenzamide](/CAS/GIF/121-81-3.gif)
121-81-3
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![3,5-Dinitrobenzonitrile](/CAS/GIF/4110-35-4.gif)
4110-35-4
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![3,5-DINITROBENZALDEHYDE](/CAS/GIF/14193-18-1.gif)
14193-18-1
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![3,5-Dinitrobenzonitrile](/CAS/GIF/4110-35-4.gif)
4110-35-4
129 suppliers
$19.00/1g