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3,6,9,12,15,18-Hexaoxanonacos-28-en-1-ol synthesis

1synthesis methods
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Yield:130727-48-9 96%

Reaction Conditions:

Stage #1: pentaethylene glycolwith sodium hydride in N,N-dimethyl-formamide at 20;Inert atmosphere;
Stage #2: 1-undecen-11-ylbromide in N,N-dimethyl-formamide at 0 - 20;Inert atmosphere;

References:

Kopitzki, Sebastian;Jensen, Knud J.;Thiem, Joachim [Chemistry - A European Journal,2010,vol. 16,# 23,p. 7017 - 7029] Location in patent:experimental part