3,6-Dichloro-1,2,4,5-tetrazine synthesis
- Product Name:3,6-Dichloro-1,2,4,5-tetrazine
- CAS Number:106131-61-7
- Molecular formula:C2Cl2N4
- Molecular Weight:150.95
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106131-61-7
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Yield:-
Reaction Conditions:
with trichloroisocyanuric acid in acetonitrile at 0 - 20; for 0.333333 h;
Steps:
5 Preparation of compound 5
Compound 4 (12.5 g, 0.09 mol) was dissolved in 350 ml of acetonitrile at 0 ° C., Add dropwise trichlorocyanuric acid(40.8 g, 0.18 mol) in acetonitrile. After the addition was completed, the mixture was warmed to room temperature for 20 minutes, then filtered. The volatiles were spun off and passed quickly through a silica gel column to give compound 5 as an orange solid.
References:
Chinese Academy Of Sciences Chemical Institute;Yang Guoqiang;Zhao Zhensheng;Wang Shuangqing;Hu Rui;Li Shayu CN107286186, 2017, A Location in patent:Paragraph 0024; 0066-0069
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106131-61-7
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106131-61-7
119 suppliers
$20.00/100mg