ChemicalBook CAS DataBase List 3,6-Dichloro-4-iodopyridazine

3,6-Dichloro-4-iodopyridazine synthesis

2synthesis methods

Product Name:3,6-Dichloro-4-iodopyridazine
CAS Number:130825-13-7
Molecular formula:C4HCl2IN2
Molecular Weight:274.87

141-30-0 Synthesis

141-30-0
395 suppliers
$6.00/10g

130825-13-7
30 suppliers
inquiry

Yield: 84%

Reaction Conditions:

Stage #1:3,6-dichlorpyridazine with zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex in tetrahydrofuran at 25; for 0.5 h;Inert atmosphere;
Stage #2: with iodine in tetrahydrofuran for 0.5 h;Inert atmosphere;

References:

Mosrin, Marc;Knochel, Paul [Organic Letters,2009,vol. 11,# 8,p. 1837 - 1840] Location in patent:supporting information; experimental part

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

130825-13-7
30 suppliers
inquiry

References

3,6-Dichloro-4-iodopyridazine Related Search:

3-METHYLBENZYLMAGNESIUM CHLORIDE 3-FLUORO-2-METHYLPHENYLMAGNESIUM BROMID& 3,5-DICHLOROPHENYLMAGNESIUM BROMIDE 3,4-DIMETHOXYPHENYLMAGNESIUM BROMIDE 3,5-Dichloropyridazine 3,5-DIMETHOXYBENZYL BROMIDE