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ChemicalBook CAS DataBase List 3,6-DICHLORO-ORTHO-ANISICACIDCHLORIDE
10411-85-5

3,6-DICHLORO-ORTHO-ANISICACIDCHLORIDE synthesis

9synthesis methods
-

Yield:10411-85-5 100%

Reaction Conditions:

Stage #1: 3,6-dichloro-2-methoxybenzoic acidwith N,N-dimethyl-formamide in dichloromethane at 0; for 0.0833333 h;
Stage #2: with oxalyl dichloride in dichloromethane at 25; for 4 h;

References:

Xiong, Wenzhang;Shi, Qiu;Liu, Wenbo H. [Journal of the American Chemical Society,2022,vol. 144,# 34,p. 15894 - 15902] Location in patent:supporting information