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ChemicalBook CAS DataBase List 3,6-DIMETHYL-3-HEPTANOL

3,6-DIMETHYL-3-HEPTANOL synthesis

3synthesis methods
-

Yield: 68.4%

Reaction Conditions:

Stage #1:i-pentyl bromide with magnesium in diethyl ether for 0.5 h;Heating;
Stage #2:butanone in diethyl ether for 2 h;Heating;Grignard reaction;

References:

Lalah, Joseph O.;Schramm, Karl-W.;Lenoir, Dieter;Henkelmann, Bernhard;Hertkorn, Norbert;Matuschek, Georg;Kettrup, Antonius;Guenther, Klaus [Chemistry - A European Journal,2001,vol. 7,# 22,p. 4790 - 4795]

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