3,7-DITHIA-1,9-NONANEDITHIOL synthesis
- Product Name:3,7-DITHIA-1,9-NONANEDITHIOL
- CAS Number:25676-62-4
- Molecular formula:C7H16S4
- Molecular Weight:228.46
16260-48-3
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25676-62-4
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Yield:25676-62-4 70%
Reaction Conditions:
Stage #1: 3,7-dithianonane-1,9-diolwith hydrogenchloride;thiourea in water; for 12 h;Reflux;
Stage #2: with potassium hydroxide in water; for 3 h;Cooling with ice;Reflux;
References:
Buter;Kellogg, Richard M. [Organic Syntheses,1987,vol. 65,p. 150 - 150]
19451-20-8
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25676-62-4
26 suppliers
$45.00/10mg