3,9-DODECADIYNE synthesis
- Product Name:3,9-DODECADIYNE
- CAS Number:61827-89-2
- Molecular formula:C12H18
- Molecular Weight:162.27
871-84-1
129 suppliers
$45.00/50mg
75-03-6
361 suppliers
$11.00/5g
61827-89-2
47 suppliers
$44.39/5g
Yield: 70%
Reaction Conditions:
Stage #1:1,7-Octadiyne with n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2:ethyl iodide with 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone in tetrahydrofuran;hexaneFurther stages.;
References:
Dumond, Yves R.;Negishi, Ei-Ichi [Tetrahedron,2004,vol. 60,# 6,p. 1345 - 1352]
