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10037-18-0

3-Acetyl-2-methyl-6-phenyl-4H-pyran-4-one synthesis

1synthesis methods
-

Yield:10037-18-0 36%

Reaction Conditions:

with dmap;1,1'-carbonyldiimidazole;sodium hydroxide;scandium tris(trifluoromethanesulfonate) in 1,2-dichloro-ethane at 80;Molecular sieve;

References:

Dong, Shuding;Fang, Chao;Tang, Weifang;Lu, Tao;Du, Ding [Organic Letters,2016,vol. 18,# 15,p. 3882 - 3885] Location in patent:supporting information